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PURIFICATION OF NANOKALSIT BASED LIMESTONE WITH COPRESIPITATION METHOD
Last modified: 2017-08-19
Abstract
Synthesis nanocalcite made of limestone using coprecipitation method has been succesfully implemented. Synthesis is held by variyng the CO2 gas pressure and precipitation time inorder to obtain calcite with high purity and small particle size. Diffraction data were collected using a X-ray diffractometer, which then analyzed using software Match and Rietica to obtain information about fitness, degree of purity, density and particle size. From analysis using Match, it was found that limestone as base material has CaCO3 and Ca(OH)2 phases, while samples which synthesized by coprecipitation method has calcite phase. Analysis result by Rietica shows that the best result is sample which synthesized with CO2 gas pressure variation of 37.5 kgf/cm3 and the settling time for 36 hours.
Keywords
limestone, calcite, coprecipitation, purity